Antioxidant BHT 264
CAS:128-37-0
Purity:99%
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Product Details
InChI:InChI=1/C12H15N/c1-12(2,3)11-6-4-10(5-7-11)8-9-13/h4-7H,8H2,1-3H3
The invention discloses a synthesis meth...
The invention discloses a method for pre...
A simple formamide catalyst facilitates ...
The present invention relates to a metho...
4-(tert-butyl)chlorobenzene

ethyl 2-cyanoacetate

4-tert-butylbenzyl cyanide
| Conditions | Yield |
|---|---|
|
ethyl 2-cyanoacetate; With potassium tert-butylate; In tert-butyl alcohol; at 98 ℃; for 0.5h; under 3420.23 Torr; Inert atmosphere;
4-(tert-butyl)chlorobenzene; In dimethyl sulfoxide; tert-butyl alcohol; at 112 ℃; for 2.5h; under 3800.26 Torr; Inert atmosphere;
With water; In dimethyl sulfoxide; tert-butyl alcohol; at 142 ℃; for 5h; under 6080.41 Torr; Temperature; Pressure; Inert atmosphere;
|
97.7% |
1-bromo-4-tert-butylbenzene

methyl 2-cyanoacetate

4-tert-butylbenzyl cyanide
| Conditions | Yield |
|---|---|
|
1-bromo-4-tert-butylbenzene; methyl 2-cyanoacetate; With sodium t-butanolate; In tetrahydrofuran; N,N-dimethyl-formamide; at 80 ℃; for 0.333333h; under 2280.15 Torr; Inert atmosphere;
In tetrahydrofuran; N,N-dimethyl-formamide; at 95 ℃; for 1h; under 3040.2 Torr; Inert atmosphere;
With water; In tetrahydrofuran; N,N-dimethyl-formamide; at 130 ℃; for 4h; under 4560.31 Torr; Inert atmosphere;
|
96.1% |
sodium cyanide
4-tert-butylbenzyl chloride
1-(bromomethyl)-4-(1,1-dimethylethyl)benzene
potassium cyanide
4-t-butylphenylacetic acid
N-[2-[4-(t-butyl)phenyl]ethyl]amine
3-(4-tert-butyl-phenyl)-3-cyano-2-oxo-propionic acid ethyl ester
dimethyl 2-methyl-2-(4-tert-butylphenyl)malonate