Antioxidant BHT 264
CAS:128-37-0
Purity:99%
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Product Details
Herein is described the development of a...
(Chemical Equation Presented) The homolo...
diethyl chloromethylphosphonate
tributyl borane
benzoyl chloride
diethyl pentylphosphonate
diethyl 1-benzoylpentylphosphonate
benzoic acid 2-(diethoxy-phosphoryl)-phenyl-hex-1-enyl ester
| Conditions | Yield |
|---|---|
|
diethyl chloromethylphosphonate; With n-butyllithium; In tetrahydrofuran; at -90 ℃; Inert atmosphere;
tributyl borane; In tetrahydrofuran; diethyl ether; at -90 - 20 ℃; Inert atmosphere;
benzoyl chloride; Further stages;
|
30% 28% 18% |
|
diethyl chloromethylphosphonate; With n-butyllithium; In tetrahydrofuran; at -90 ℃; Inert atmosphere;
tributyl borane; In tetrahydrofuran; diethyl ether; at -90 - 20 ℃; Inert atmosphere;
benzoyl chloride; Further stages;
|
44 %Spectr. 4 %Spectr. 52 %Spectr. |
1-Bromopentane
triethyl phosphite
ethylphosphonic acid diethyl ester
diethyl pentylphosphonate
| Conditions | Yield |
|---|---|
|
In neat (no solvent); at 260 ℃; for 0.0166667h; under 25858.1 Torr; Temperature; Flow reactor;
|
|
|
In neat (no solvent); at 300 ℃; for 0.0166667h; under 25858.1 Torr; Temperature; Flow reactor;
|
diethyl chloromethylphosphonate
tributyl borane
benzoyl chloride
1-Bromopentane
pentyl-phosphonic acid ethyl ester-(4-nitro-phenyl ester)
