Antioxidant BHT 264
CAS:128-37-0
Purity:99%
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Product Details
|
Uses |
3-Methyl-5-(phenylmethoxy)-2-[4-(phenylmethoxy)phenyl]-1H-indole is an intermediate of Bazedoxifene acetate (B129250). |
InChI:InChI=1/C29H25NO2/c1-21-27-18-26(32-20-23-10-6-3-7-11-23)16-17-28(27)30-29(21)24-12-14-25(15-13-24)31-19-22-8-4-2-5-9-22/h2-18,30H,19-20H2,1H3
A series of 3-methyl-2-phenyl-1H-indoles...
We report here cobalt-N-heterocyclic car...
A genus of proteolysis-targeting chimera...
The invention relates to a process for p...
1-<4-(benzyloxy)phenyl>-2-bromo-1-propanone
4-benzyloxyaniline hydrochloride
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
| Conditions | Yield |
|---|---|
|
With
triethylamine;
In
N,N-dimethyl-formamide;
at 115 ℃;
for 4h;
Temperature;
Reagent/catalyst;
|
94.6% |
|
1-<4-(benzyloxy)phenyl>-2-bromo-1-propanone; 4-benzyloxyaniline hydrochloride;
With
triethylamine;
In
butan-1-ol;
at 118 ℃;
for 3h;
With
hydrogenchloride;
In
water; butan-1-ol;
at 118 ℃;
for 7h;
Temperature;
Reagent/catalyst;
|
90.5% |
|
With
triethylamine;
In
N,N-dimethyl-formamide;
at 120 - 150 ℃;
for 4h;
Inert atmosphere;
|
84.9% |
|
With
triethylamine;
In
N,N-dimethyl-formamide;
at 100 - 125 ℃;
|
65.14% |
|
With
triethylamine;
In
N,N-dimethyl-formamide;
Heating;
|
51% |
|
With
triethylamine;
In
N,N-dimethyl-formamide;
at 120 - 150 ℃;
for 4.66667h;
|
|
|
With
triethylamine;
In
N,N-dimethyl-formamide;
at 120 - 150 ℃;
for 5h;
|
C33H27N3O2
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
| Conditions | Yield |
|---|---|
|
With
sodium ethanolate;
In
ethanol; dimethyl sulfoxide;
at 100 ℃;
for 20h;
|
85% |
|
With
sodium ethanolate;
In
dimethyl sulfoxide;
at 130 ℃;
|
72% |
1-<4-(benzyloxy)phenyl>-2-bromo-1-propanone
4-benzyloxyaniline hydrochloride
p-benzyloxyaniline
1-(4-benzyloxyphenyl)-2-(4-benzyloxy-phenylamino)-1-propanone
{4-[5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-indol-1-ylmethyl]-phenoxy}-acetic acid ethyl ester
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1-[4-(2-pyrrolidin-1-yl-propoxy)-benzyl]-1H-indole
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1-{4-[2-(3-methyl-pyrrolidin-1-yl)-ethoxy]-benzyl}-1H-indole
5-Benzyloxy-2-(4-benzyloxy-phenyl)-1-[4-(3-chloro-propoxy)-benzyl]-3-methyl-1H-indole
