Antioxidant BHT 264
CAS:128-37-0
Purity:99%
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Product Details
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Purification Methods |
Purify the ester by repeated crystallisation, from hexane, of its addition compound with uranyl nitrate. Decompose the complex, and distil the ester at high vacuum. [Siddall J Am Chem Soc 81 4176 1959.] [see tributyl phosphate and Cherbuliez in Organo Phosphorus Compounds (Kosolapoff & Maier eds) Wiley Vol 6 pp 211-577 1973.] |
InChI:InChI=1/C15H33O4P/c1-13(2)7-10-17-20(16,18-11-8-14(3)4)19-12-9-15(5)6/h13-15H,7-12H2,1-6H3
Trialkylphosphates are synthesized from ...
Oxidative alkoxylation of Zn3P2 with the...
Sodium hypophosphite oxidazies in alcoho...
Trialkyl phosphates are rapidly and sele...
i-Amyl alcohol
triisoamyl phosphate
1-chloro-3-methylbutane
| Conditions | Yield |
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With zinc(II) phosphide; oxygen; copper dichloride; at 60 ℃; under 750.06 Torr; Title compound not separated from byproducts;
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92.8% |
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With phosphan; chlorine; at 20 ℃; Rate constant; Thermodynamic data; Ea, ΔS(excit.); var. temp.; also in the presence of pyridine;
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With zinc(II) phosphide; oxygen; copper dichloride; at 60 ℃; Kinetics;
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hydrogenchloride
zinc(II) phosphide
i-Amyl alcohol
oxygen
diisoamylphosphoric acid
triisoamyl phosphate
1-chloro-3-methylbutane
zinc(II) chloride
| Conditions | Yield |
|---|---|
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copper dichloride; In further solvent(s); Kinetics;
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i-Amyl alcohol
hydrogenchloride
oxygen
