3871-20-3

  • Product Name:TRIS(4-NITROPHENYL) PHOSPHATE
  • Molecular Formula:C18H12 N3 O10 P
  • Purity:99%
  • Molecular Weight:461.281
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Product Details

  • CasNo: 3871-20-3
  • Molecular Formula: C18H12 N3 O10 P
  • Chinese Factory Supply Wholesale TRIS(4-NITROPHENYL) PHOSPHATE 3871-20-3 On Stock

    • Molecular Formula:C18H12 N3 O10 P
    • Molecular Weight:461.281
    • Melting Point:156-158 °C
       
    • Boiling Point:592°Cat760mmHg 
    • Flash Point:311.8°C 
    • PSA:192.03000 
    • Density:1.572g/cm3 
    • LogP:6.62570 

    TRIS(4-NITROPHENYL) PHOSPHATE(Cas 3871-20-3) Usage

    Chemical Properties

    Light yellow powder

    Purification Methods

    It has been recrystallised from AcOH, dioxane, AcOEt and Me2CO and dried it in a vacuum over P2O5. [Katelaar & Gersmann J Am Chem Soc 72 5777 1950, Moffatt & Khorana J Am Chem Soc 79 3741 1957.]

    InChI:InChI=1/C18H12N3O10P/c22-19(23)13-1-7-16(8-2-13)29-32(28,30-17-9-3-14(4-10-17)20(24)25)31-18-11-5-15(6-12-18)21(26)27/h1-12H

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    3871-20-3 Process route

    4-nitro-phenol
    100-02-7,78813-13-5,89830-32-0

    4-nitro-phenol

    tris(p-nitrophenyl)phosphate
    3871-20-3

    tris(p-nitrophenyl)phosphate

    4-chlorobenzonitrile
    100-00-5

    4-chlorobenzonitrile

    Conditions
    Conditions Yield
    With phosphorus pentachloride;
    4-nitro-phenol
    100-02-7,78813-13-5,89830-32-0

    4-nitro-phenol

    tris(p-nitrophenyl)phosphate
    3871-20-3

    tris(p-nitrophenyl)phosphate

    Conditions
    Conditions Yield
    4-nitro-phenol; With sodium; In methanol; toluene; at 30 - 45 ℃;
    With trichlorophosphate; In toluene; for 0.0833333h; Thermodynamic data; Kinetics;
    95%
    With triethylamine; trichlorophosphate; In acetonitrile; at 20 ℃; for 1.16667h; Cooling with ice;
    77.6%
    With triethylamine; trichlorophosphate; In acetonitrile; at 20 ℃; for 1.166h; Inert atmosphere; Cooling with ice;
    With pyridine; trichlorophosphate; In toluene; at 110 ℃; for 4h;
    4-nitro-phenol; With sodium methylate; In methanol; toluene; Heating;
    With trichlorophosphate; In toluene; at 45 ℃; Temperature; Time; Kinetics;
    With trichlorophosphate;
    4-nitro-phenol; With triethylamine; In acetonitrile; Inert atmosphere;
    With trichlorophosphate; In acetonitrile; at 0 - 20 ℃; for 1.16667h; Inert atmosphere;

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    CAS:128-37-0

    Purity:99%

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