Antioxidant BHT 264
CAS:128-37-0
Purity:99%
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Product Details
| 
                             Chemical Properties  | 
             			Light yellow powder  | 
             		
| 
                             Purification Methods  | 
             			It has been recrystallised from AcOH, dioxane, AcOEt and Me2CO and dried it in a vacuum over P2O5. [Katelaar & Gersmann J Am Chem Soc 72 5777 1950, Moffatt & Khorana J Am Chem Soc 79 3741 1957.]  | 
             		
InChI:InChI=1/C18H12N3O10P/c22-19(23)13-1-7-16(8-2-13)29-32(28,30-17-9-3-14(4-10-17)20(24)25)31-18-11-5-15(6-12-18)21(26)27/h1-12H
Phosphates and phosphonates compounds of...
We report the targeted decomposition of ...
The present invention refers to novel fl...
The invention discloses a process for pr...
                                            
                                        4-nitro-phenol
                                
                                            
                                        tris(p-nitrophenyl)phosphate
                                
                                            
                                        4-chlorobenzonitrile
| Conditions | Yield | 
|---|---|
| 
                                        
                                         
                                            
                                                
                                            
                                            With 
                                            
                                            
                                                
                                                    phosphorus pentachloride; 
                                            
                                            
                                                
                                            
                                            
                                                
                                            
                                         
                                        
                                     | 
                                    
                                            
                                        4-nitro-phenol
                                
                                            
                                        tris(p-nitrophenyl)phosphate
| Conditions | Yield | 
|---|---|
| 
                                        
                                         
                                            
                                                4-nitro-phenol; 
                                            
                                            With 
                                            
                                            
                                                
                                                    sodium; 
                                            
                                            
                                                
                                            
                                            In 
                                            
                                                methanol; toluene; 
                                            
                                            
                                            
                                                
                                                            at 30 - 45 ℃;
                                                            
                                            
                                         
                                        
                                        
                                            
                                                
                                            
                                            With 
                                            
                                            
                                                
                                                    trichlorophosphate; 
                                            
                                            
                                                
                                            
                                            In 
                                            
                                                toluene; 
                                            
                                            
                                            
                                                
                                                            for 0.0833333h;
                                                            
                                                Thermodynamic data;
                                                            
                                                Kinetics;
                                                            
                                            
                                         
                                        
                                     | 
                                    
                                        95% | 
                                
| 
                                        
                                         
                                            
                                                
                                            
                                            With 
                                            
                                            
                                                
                                                    triethylamine; trichlorophosphate; 
                                            
                                            
                                                
                                            
                                            In 
                                            
                                                acetonitrile; 
                                            
                                            
                                            
                                                
                                                            at 20 ℃;
                                                            
                                                            for 1.16667h;
                                                            
                                                Cooling with ice;
                                                            
                                            
                                         
                                        
                                     | 
                                    
                                        77.6% | 
                                
| 
                                        
                                         
                                            
                                                
                                            
                                            With 
                                            
                                            
                                                
                                                    triethylamine; trichlorophosphate; 
                                            
                                            
                                                
                                            
                                            In 
                                            
                                                acetonitrile; 
                                            
                                            
                                            
                                                
                                                            at 20 ℃;
                                                            
                                                            for 1.166h;
                                                            
                                                Inert atmosphere;
                                                            
                                                Cooling with ice;
                                                            
                                            
                                         
                                        
                                     | 
                                    |
| 
                                        
                                         
                                            
                                                
                                            
                                            With 
                                            
                                            
                                                
                                                    pyridine; trichlorophosphate; 
                                            
                                            
                                                
                                            
                                            In 
                                            
                                                toluene; 
                                            
                                            
                                            
                                                
                                                            at 110 ℃;
                                                            
                                                            for 4h;
                                                            
                                            
                                         
                                        
                                     | 
                                    |
| 
                                        
                                         
                                            
                                                4-nitro-phenol; 
                                            
                                            With 
                                            
                                            
                                                
                                                    sodium methylate; 
                                            
                                            
                                                
                                            
                                            In 
                                            
                                                methanol; toluene; 
                                            
                                            
                                            
                                                
                                                Heating;
                                                            
                                            
                                         
                                        
                                        
                                            
                                                
                                            
                                            With 
                                            
                                            
                                                
                                                    trichlorophosphate; 
                                            
                                            
                                                
                                            
                                            In 
                                            
                                                toluene; 
                                            
                                            
                                            
                                                
                                                            at 45 ℃;
                                                            
                                                Temperature;
                                                            
                                                Time;
                                                            
                                                Kinetics;
                                                            
                                            
                                         
                                        
                                     | 
                                    |
| 
                                        
                                         
                                            
                                                
                                            
                                            With 
                                            
                                            
                                                
                                                    trichlorophosphate; 
                                            
                                            
                                                
                                            
                                            
                                                
                                            
                                         
                                        
                                     | 
                                    |
| 
                                        
                                         
                                            
                                                4-nitro-phenol; 
                                            
                                            With 
                                            
                                            
                                                
                                                    triethylamine; 
                                            
                                            
                                                
                                            
                                            In 
                                            
                                                acetonitrile; 
                                            
                                            
                                            
                                                
                                                Inert atmosphere;
                                                            
                                            
                                         
                                        
                                        
                                            
                                                
                                            
                                            With 
                                            
                                            
                                                
                                                    trichlorophosphate; 
                                            
                                            
                                                
                                            
                                            In 
                                            
                                                acetonitrile; 
                                            
                                            
                                            
                                                
                                                            at 0 - 20 ℃;
                                                            
                                                            for 1.16667h;
                                                            
                                                Inert atmosphere;
                                                            
                                            
                                         
                                        
                                     | 
                                    
                                4-nitro-phenol
                                phosphoric acid triphenyl ester
                                4-(4-nitrophenoxy)butanoic acid
                                potassium 4-nitrophenolate
                                triethyl phosphate
                                bis(4-nitrophenyl) ethyl phosphate
                                1-nitro-4-octyloxybenzene
                                benzyl 4-nitrophenyl ether